Response | Source | Sum of square | df | Mean square | Value F | Prob F |
---|---|---|---|---|---|---|
Model | 46.23 | 9 | 5.14 | 14.35 | 0.0001*** | |
x1 | 9.03 | 1 | 9.03 | 25.21 | 0.0005*** | |
x2 | 2.4 | 1 | 2.4 | 6.71 | 0.0270** | |
x3 | 21.61 | 1 | 21.61 | 60.37 | < 0.0001*** | |
x1x2 | 0.08 | 1 | 0.08 | 0.2235 | 0.6465 ns | |
x1x3 | ||||||
x2x3 | 7.22 | 1 | 7.22 | 20.17 | 0.0012*** | |
x1x2 | ||||||
WVP (10–11 g/m s Pa) | x2x3 | 0.125 | 1 | 0.125 | 0.3492 | 0.5677 ns |
x12 | 2.16 | 1 | 2.16 | 6.04 | 0.0339** | |
x22 | 0.0005 | 1 | 0.0005 | 0.0014 | 0.9706 ns | |
x32 | 0.2255 | 1 | 0.2255 | 0.63 | 0.4458 ns | |
Residual | 3.58 | 10 | 0.3579 | |||
Lack of Fit | 2.03 | 5 | 0.4052 | 0.3889 ns | ||
Pure Error | 1.55 | 5 | 0.3107 | |||
Model | 825.66 | 9 | 91.74 | 24.01 | < 0.0001*** | |
x1 | 511.23 | 1 | 511.23 | 133.8 | < 0.0001*** | |
x2 | 54.76 | 1 | 54.76 | 14.33 | 0.0036*** | |
x3 | 120.41 | 1 | 120.41 | 31.51 | 0.0002*** | |
x1x2 | 0.6612 | 1 | 0.6612 | 0.1731 | 0.6862 ns | |
x1x3 | ||||||
Solubility (%) | x2x3 | 43.71 | 1 | 43.71 | 11.44 | 0.0070*** |
x1x2 | 3.25 | 1 | 3.25 | 0.8509 | 0.3780 ns | |
x2x3 | ||||||
x12 | 61.22 | 1 | 61.22 | 16.02 | 0.0025*** | |
x22 | 3.75 | 1 | 3.75 | 0.9822 | 0.3450 ns | |
x32 | 21.28 | 1 | 21.28 | 5.57 | 0.0400** | |
Residual | 38.21 | 10 | 3.82 | |||
Lack of Fit | 27.95 | 5 | 5.59 | 2.73 | 0.1476 ns | |
Pure Error | 10.26 | 5 | 2.05 | |||
Model | 27.2 | 9 | 3.02 | 9.05 | 0.0010*** | |
x1 | 2.21 | 1 | 2.21 | 6.61 | 0.0278** | |
x2 | 4.23 | 1 | 4.23 | 12.65 | 0.0052*** | |
x3 | 12.77 | 1 | 12.77 | 38.22 | 0.0001*** | |
x1x2 | 0.845 | 1 | 0.845 | 2.53 | 0.1428 ns | |
x1x3 | ||||||
Tensile Strength (MPa) | x2x3 | 2.21 | 1 | 2.21 | 6.6 | 0.0279** |
x1x2 | 0.845 | 1 | 0.845 | 2.53 | 0.1428 ns | |
x2x3 | ||||||
x12 | 0.4009 | 1 | 0.4009 | 1.2 | 0.2990 ns | |
x22 | 0.0384 | 1 | 0.0384 | 0.115 | 0.7416 ns | |
x32 | 2.85 | 1 | 2.85 | 8.53 | 0.0153** | |
Residual | 3.34 | 10 | 0.3341 | |||
Lack of Fit | 0.9661 | 5 | 0.1932 | 0.4068 | 0.8270 ns | |
Pure Error | 2.38 | 5 | 0.475 | |||
Model | 737.21 | 9 | 81.91 | 26.07 | < 0.0001*** | |
x1 | 205.21 | 1 | 205.21 | 65.3 | < 0.0001*** | |
x2 | 19.6 | 1 | 19.6 | 6.24 | 0.0316** | |
x3 | 297.03 | 1 | 297.03 | 94.52 | < 0.0001*** | |
x1x2 | 4.65 | 1 | 4.65 | 1.48 | 0.2517 ns | |
x1x3 | ||||||
Elongation (%) | x2x3 | 116.28 | 1 | 116.28 | 37 | 0.0001*** |
x1x2 | 1.9 | 1 | 1.9 | 0.605 | 0.4547 ns | |
x2x3 | ||||||
x12 | 18.14 | 1 | 18.14 | 5.77 | 0.0372** | |
x22 | 0.1309 | 1 | 0.1309 | 0.0417 | 0.8424 ns | |
x32 | 11.76 | 1 | 11.76 | 3.74 | 0.0818 ns | |
Residual | 31.42 | 10 | 3.14 | |||
Lack of Fit | 19.61 | 5 | 3.92 | 1.66 | 0.2958 ns | |
Pure Error | 11.81 | 5 | 2.36 | |||
Model | 0.0196 | 6 | 0.0033 | 17.21 | < 0.0001*** | |
x1 | 0.013 | 1 | 0.013 | 68.42 | < 0.0001*** | |
x2 | 0.0003 | 1 | 0.0003 | 1.32 | 0.2713 ns | |
x3 | 0.0044 | 1 | 0.0044 | 23.28 | 0.0003*** | |
Thickness (mm) | x1x2 | 0.0006 | 1 | 0.0006 | 3.23 | 0.0954 ns |
x1x3 | 0.001 | 1 | 0.001 | 5.35 | 0.0378** | |
x2x3 | ||||||
x1x2 | 0.0003 | 1 | 0.0003 | 1.65 | 0.2214 ns | |
x2x3 | ||||||
Residual | 0.0025 | 13 | 0.0002 | |||
Lack of Fit | 0.0011 | 8 | 0.0001 | 0.5293 | 0.7980 ns | |
Pure Error | 0.0013 | 5 | 0.0003 | |||
Model | 3338.08 | 9 | 370.9 | 92.61 | < 0.0001*** | |
x1 | 26.24 | 1 | 26.24 | 6.55 | 0.0284** | |
x2 | 1.16 | 1 | 1.16 | 0.2886 | 0.6028 ns | |
x3 | 3083.54 | 1 | 3083.54 | 769.94 | < 0.0001*** | |
x1x2 | 1.81 | 1 | 1.81 | 0.4507 | 0.5172 ns | |
x1x3 | ||||||
Antioxidant activity (%) | x2x3 | 19.22 | 459930524115395001 | 19.22 | 4.8 | 0.0533 ns |
x1x2 | 0.605 | 1 | 0.605 | 0.1511 | 0.7057 ns | |
x2x3 | ||||||
x12 | 14.43 | 1 | 14.43 | 3.6 | 0.0869 ns | |
x22 | 0.1202 | 1 | 0.1202 | 0.03 | 0.8659 ns | |
x32 | 150.96 | 1 | 150.96 | 37.69 | 0.0001*** | |
Residual | 40.05 | 10 | 4 | |||
Lack of Fit | 13.34 | 5 | 2.67 | 0.4992 | 0.7680 ns | |
Pure Error | 26.71 | 5 | 5.34 |