Solvent effects on terpenoid compositions and antioxidant activities of Cinnamomum camphora (L.) J. Presl extracts and the main antioxidant agent evaluation through in vitro and in vivo assay

Wang, Yingying; Zhang, Siyi; Ma, Yuandan; Du, Xianmin; Zong, Qi; Lin, Die; Lai, Meng; Huang, Tianyu; Luo, Qingyun; Yang, Lin; Li, Zhanyong; Zuo, Zhaojiang

doi:10.1186/s40538-023-00524-2

Chemical and Biological Technologies in Agriculture

Table 2 The main terpenoids in different extracts from the eucalyptol chemotype of C. camphora

From: Solvent effects on terpenoid compositions and antioxidant activities of Cinnamomum camphora (L.) J. Presl extracts and the main antioxidant agent evaluation through in vitro and in vivo assay

Retention time (min)	Terpenoids	Formula	MeOH extracts (µM)	EA extracts (µM)	Hex extracts (µM)	PE extracts (µM)
6.450	β-Thujene	C₁₀H₁₆	21.34 ± 6.25	15.12 ± 1.58	17.18 ± 2.34	16.48 ± 2.85
6.536	α-Pinene	C₁₀H₁₆	42.07 ± 2.70	29.83 ± 2.45	27.27 ± 2.41	22.68 ± 5.99
6.712	Camphene	C₁₀H₁₆	3.31 ± 0.64	1.72 ± 0.41	1.52 ± 0.15	1.33 ± 0.46
6.970	β-Phellandrene	C₁₀H₁₆	146.09 ± 19.91	131.55 ± 13.34	126.05 ± 23.97	106.50 ± 4.59
7.006	β-Pinene	C₁₀H₁₆	45.63 ± 0.94	28.94 ± 3.09	37.94 ± 6.65	29.95 ± 3.55
7.114	Myrcene	C₁₀H₁₆	23.46 ± 1.86	19.75 ± 4.34	20.73 ± 3.59	20.43 ± 1.72
7.282	α-Phellandrene	C₁₀H₁₆	1.82 ± 0.72	0.74 ± 0.05	1.25 ± 0.19	1.02 ± 0.39
7.401	α-Terpinene	C₁₀H₁₆	2.64 ± 0.36	2.27 ± 0.11	2.50 ± 0.19	2.31 ± 0.23
7.526	D-Limonene	C₁₀H₁₆	130.45 ± 15.57	82.22 ± 4.39	90.55 ± 12.14	108.42 ± 8.22
7.573	Eucalyptol	C₁₀H₁₈O	3143.39 ± 157.36	2232.34 ± 65.61	2125.91 ± 102.8	1820.53 ± 55.99
7.663	Ocimene	C₁₀H₁₆	6.69 ± 0.25	4.91 ± 0.23	5.83 ± 1.29	4.98 ± 0.45
7.792	γ-Terpinene	C₁₀H₁₆	24.07 ± 2.23	16.04 ± 3.66	13.31 ± 2.34	11.49 ± 0.71
7.889	β-Terpineol	C₁₀H₁₈O	122.92 ± 14.65	118.91 ± 15.99	101.71 ± 16.65	88.19 ± 1.03
8.065	2-Carene	C₁₀H₁₆	10.14 ± 0.87	8.72 ± 0.34	7.69 ± 0.66	5.32 ± 1.61
8.133	Linalool	C₁₀H₁₈O	3.39 ± 0.26	2.35 ± 0.25	1.81 ± 0.35	2.16 ± 0.18
8.377	Fenchene	C₁₀H₁₆	2.82 ± 0.28	2.58 ± 0.32	2.11 ± 0.54	2.44 ± 0.41
8.768	Borneol	C₁₀H₁₈O	59.15 ± 3.85	47.03 ± 3.19	42.49 ± 3.18	37.39 ± 3.03
8.843	Myrcenol	C₁₀H₁₈O	30.87 ± 4.44	27.60 ± 4.77	26.88 ± 4.92	26.52 ± 2.13
8.951	α-Terpineol	C₁₀H₁₈O	687.20 ± 2.27	567.37 ± 8.98	486.50 ± 35.91	537.25 ± 26.79
9.974	δ-Elemene	C₁₅H₂₄	3.43 ± 0.46	2.03 ± 0.15	2.72 ± 0.24	2.47 ± 0.59
10.042	Elixene	C₁₅H₂₄	29.20 ± 4.69	19.28 ± 0.56	20.65 ± 4.78	22.59 ± 0.72
10.347	α-Copaene	C₁₅H₂₄	1.75 ± 0.09	1.73 ± 0.22	1.67 ± 0.59	1.48 ± 0.12
10.444	β-Elemene	C₁₅H₂₄	8.01 ± 0.24	7.96 ± 0.37	7.65 ± 2.34	6.55 ± 0.76
10.652	Longifolene	C₁₅H₂₄	71.06 ± 9.35	66.09 ± 3.34	55.35 ± 1.74	57.29 ± 5.28
10.760	γ-Elemene	C₁₅H₂₄	4.19 ± 0.56	3.42 ± 0.52	4.06 ± 0.39	3.76 ± 0.33
11.011	Humulene	C₁₅H₂₄	39.10 ± 2.41	29.26 ± 2.96	31.42 ± 0.90	30.47 ± 8.02
11.197	Germacrene	C₁₅H₂₄	8.52 ± 0.59	2.14 ± 0.07	3.43 ± 0.67	3.40 ± 0.05
11.237	cis-β-Copaene	C₁₅H₂₄	12.38 ± 0.87	11.08 ± 0.17	11.54 ± 2.43	11.48 ± 0.92
11.301	β-Eudesmen	C₁₅H₂₄	8.98 ± 1.45	6.16 ± 0.45	7.81 ± 2.11	7.11 ± 0.62
11.380	Bicyclogermacrene	C₁₅H₂₄	44.02 ± 7.11	41.01 ± 1.93	29.12 ± 1.48	38.29 ± 0.86
11.578	δ-Cadinene	C₁₅H₂₄	2.79 ± 0.33	3.15 ± 0.59	2.60 ± 0.24	2.42 ± 0.04
11.887	Elemol	C₁₅H₂₆O	1.59 ± 0.17	1.07 ± 0.09	1.45 ± 0.12	1.24 ± 0.08
12.034	γ-Patchoulene	C₁₅H₂₄	1.51 ± 0.16	1.22 ± 0.31	0.91 ± 0.02	1.39 ± 0.13
13.261	Viridiflorol	C₁₅H₂₆O	4.31 ± 0.48	2.40 ± 0.17	1.70 ± 0.05	2.05 ± 0.36

MeOH Methanol, EA Ethyl acetate, Hex n-Hexane, PE Petroleum ether. Means ± SE (n = 4)

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