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Table 3 HMBC and NOESY spectrum assignments for LP-1

From: Structural characterization of a low-molecular weight linear O-acetyl-glucomannan in Lilium lancifolium from Tibet and its protected H2O2-induced oxidative stress in HUVEC cells

Connection mode

B → E

E → C

C → E

E → E

E → D

D → D

D → E

D → A

H1

Cn

–

4.41

77.60

4.85

79.46

–

4.41

77.93

4.67

77.93

4.67

79.46

4.67

81.91

C1

Hn

100.41

3.58

–

101.46

3.58

103.90

3.58

–

100.94

3.71

100.94

3.58

100.94

3.95

H1

Hn

5.33

3.58

4.41

3.78

4.85

3.58

4.41

3.58

4.41

3.71

4.67

3.71

4.67

3.58

4.67

3.95

  1. – Not detected