From: Chemical and spectroscopic characterization of insoluble and soluble humic acid fractions at different pH values
Fraction
1H NMR distribution (%)
0.5 to 3.0 ppm
3.0 to 4.2 ppm
6.0 to 8.0 ppm
pH 5
Insoluble
45.6
36.7
17.7
Soluble
45.2
23.2
31.6
pH 7
47.6
40.3
12.1
46.9
20.5
32.6