No | 3 | 4 | ||
---|---|---|---|---|
δC | δH (J in Hz) | δC | δH (J in Hz) | |
1 | 167.5 (C) | 166.3 (C) | ||
3 | 44.2 (CH2) | 4.24, s | 39.7 (CH2) | 4.21, s |
4 | 156.8 (C) | 156.8 (C) | ||
5 | 123.9 (C) | 123.7 (C) | ||
6 | 152.2 (C) | 152.4 (C) | ||
7 | 115.7 (CH) | 7.48, s | 115.4 (CH) | 7.50, s |
3a | 125.1 (C) | 125.4 (C) | ||
7a | 136.7 (C) | 136.8 (C) | ||
8 | 28.2 (CH2) | 2.68, t (5.6) | 28.2 (CH2) | 2.68, t (5.6) |
9 | 37.4 (CH2) | 3.36, t (5.6) | 37.2 (CH2) | 3.36, t (5.6) |
10 | 206.3 (C) | 206.3 (C) | ||
4-OMe | 60.9 (CH3) | 3.82, s | 60.9 (CH3) | 3.84, s |
2′ | 153.2 (C) | 161.7 (C) | ||
3′ | 121.6 (CH) | 6.94, d (7.8) | 114.6 (CH) | 6.74, d (8.8) |
4′ | 122.4 (CH) | 7.04, d (7.8) | 144.6 (CH) | 7.59, d (8.8) |
5′ | 154.4 (C) | 118.2 (C) | ||
6′ | 145.9 (C) | 155.6 (C) | ||
7′ | 32.1 (CH2) | 3.16, t (6.2) | 52.3 (CH2) | 4.02, s |
8′ | 46.8 (CH2) | 3.56, t (6.2) | 14.2 (CH3) | 2.21, s |
9′ | 18.3 (CH3) | 2.32, s | ||
5′-OMe | 55.9 (CH3) | 3.80, s | ||
1′-NH | 8.90, s |