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Table 2 1H and 13C NMR chemical shifts of PSRa-2

From: Structural properties and immunomodulatory activity of an α-glucan purified from the fruiting body of Stropharia rugosoannulata

Code

Glycosyl residues

Chemical shifts (ppm)

H1/C1

H2/C2

H3/C3

H4/C4

H5/C5

H6/C6

A

→4)-α-d-Glcp-(1→

5.34

3.55

3.96

3.59

3.89

3.79, 3.61

99.77

71.65

69.57

77.05

73.36

60.54

B

→3)-α-d-Glcp-(1→

4.93

3.78

3.49

3.64

3.53

3.85, 3.71

97.87

68.3

78.69

72.68

67.28

60.57

C

α-d-Glcp-(1→

5.08

3.89

3.77

3.36

3.82

3.77

98.37

73.36

71.31

69.45

69.7

60.48

D

→4,6)-α-d-Glcp-(1→

5.31

3.57

3.95

3.58

3.9

3.85, 3.64

99.87

71.87

69.45

77.18

73.36

66.56